Determination of purity of methacrylic acid by a titration method with 1(N) sodium hydroxide (NaOH) solution and using in Phenolphthalein indicator solution.
APPARATUS
a). 5 ml stoppered weighing bottle.
b). 250 ml conical flask.
c). 100 ml measuring cylinder.
d). Burette.
REAGENTS
a). Standard 1(N) sodium hydroxide (NaOH) solution.
b). Phenolphthalein indicator solution.
PROCEDURE
Take a Methacrylic acid sample in a 5 ml stoppered weighing bottle. From this carefully transfer about 1 gm (weighing accurately) sample into a 250-ml conical flask.Â
Add about 100-ml distilled water and shake well to mix properly. Titrate against standard 1(N) sodium hydroxide (NaOH) solution taken in a burette using phenolphthalein as indicator.
Calculation of PurityÂ
Assay (%) = Titre value (ml) x normality of NaOH x 8.609 / Wt of Methacrylic acid sample taken (gm)
Methacrylic acid Formula
Methacrylic acid chemical Formula is C4H6O2.
Use Of Methacrylic Acid
Mainly used methacrylic acid is in paints, adhesives, and leather treatment agents, making plastic sheets and other organic chemicals methacrylic acid is also used as a raw material in the manufacture of ion-exchange resins.
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